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Trilithium aluminium trimolybdate(VI), Li3Al(MoO4)3, has been grown as single crystals from α‐Al2O3 and MoO3 in an Li2MoO4 flux at 998 K. This compound is an example of the well known lyonsite structure type, the general formula of which can be written as A16B12O48. Because this structure can accomodate cationic mixing as well as cationic vacancies, a wide range of chemical compositions can adopt...
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