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The sol–gel combustion synthesis (SGCS) for oxygen carrier (OC) to be used in chemical looping combustion (CLC) was first designed and experimented in this work, which is a new method of OC synthesis by combining sol–gel technique and solution combustion synthesis. Cheap hydrated metal nitrates and urea were adopted as precursors to prepare Fe 2 O 3 /Al 2 O 3 OC at...
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