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Hybrid inorganic–organic framework materials exhibit unique properties that can be advantageously tuned through choice of the inorganic and organic components and by control of the crystal structure. We present a new hydrothermally prepared 3D hybrid framework, [Mn(2‐methylsuccinate)]n (1), comprising alternating 2D manganese oxide sheets and isolated MnO6 octahedra, pillared via syn, anti–syn carboxylates...
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