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Nanocrystalline copper–cobalt ferrites with composition Cu1−xCoxFe2O4, where x = 0.2 and 0.8, were synthesized by mechanochemical treatment of co-precipitated precursors. The ferrite powders were characterized by XRD and Mössbauer spectroscopy. Results proved obtaining of spinel ferrites with crystallite size smaller than 10 nm. Increasing of crystallite size of samples with increasing of mechanochemical...
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