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A complete chromium depletion profile with its depth resolution in the nanometre range was obtained on a Ni–16Cr–9Fe model alloy after a 10h oxidation at 950°C in air. Auger electron spectroscopy coupled to ion sputtering and energy-dispersive X-ray spectroscopy were used to measure the chromium depletion profile. The chromium content at the oxide/alloy interface is below 0.5wt.%. This exceptionally...
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