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Hydroxyborohydride (sodium and potassium salts) were prepared by a one-pot method and the 1 H NMR spectrum of sodium hydroxyborohydride was recorded for the first time. Based on an NMR experiment, hydroxyborohydride was found to be more reactive toward acetone carbonyl than borohydride. The calculated 11 B- and 10 B–H coupling constants are in very good agreement with experimental...
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