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A nanostructured anatase supported V-O-Mo catalyst with V:Mo:Ti=1:9:90, obtained by sol-gel method from inorganic substrates, was investigated. The structure of the species formed on the catalyst surface in the course of synthesis was determined and its evolution during oxidation and reduction was studied by the FT Raman spectroscopy. Vanadia-like monolayer islands with some molybdenum atoms substituted...
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