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Ni–Fe alloys obtained by high energy ball milling of pure Ni and Fe powders were investigated by 57 Fe Mössbauer spectrometry. The Mössbauer spectra of the as-milled powders were fitted with two magnetic contributions, corresponding to the α-Fe and Ni–Fe phases. As the milling time increases, the relative intensity of the α-Fe contribution decreases while that of the Ni–Fe phase increases...
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