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•Fe 60 Co 40 alloy nanoparticles with an average particle size of 30nm were successfully synthesized in gram scale batches using the modified polyol process.•Fe 60 Co 40 alloy nanoparticles are not available commercially even in gram scale quantities.•The saturation magnetization for the gram scale synthesized Fe 60 Co 40 alloy nanoparticles is in the...
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