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In situ micro-FTIR spectroscopy was explored to characterize the solid–solid interface between lithium electrode and polymer electrolytes. The cyclic voltammetric (CV) results indicated that the reduction reactions of oxygen and water as well as the formation of underpotential deposition (UPD) Li occur in the Li/PEO 20 -LiN(CF 3 SO 2 ) 2 electrolyte interface in the...
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