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The synthesis, characterization, and detailed thermal properties of N-alkylpiperidine·alane compounds are described. Direct reaction of 1 equiv of N-alkylpiperidine (NMPi or NEPi, NMPi = N-methylpiperidine, NEPi = N-ethylpiperidine) with 1 equiv of γ-AlH 3 readily gives the 1:1 adduct NMPi·AlH 3 (or NEPi·AlH 3 ) in good yields and purity. Attempts to prepare the related 2:1...
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