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A novel method for preparation of ZrB2 coatings has been proposed by combination of molten salt synthesis of ZrB2 nanoparticles and subsequent electrophoretic deposition of the as‐synthesized ZrB2 nanoparticles in the same molten system in this paper. Nanoscale ZrB2 particles have been produced by borothermal reduction of ZrO2 in NaCl‐KCl‐AlF3 melt at 980°C. Then electrophoretic deposition of the...