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The reaction of Os3(CO)10(NCMe)2 with closo‐o‐C2B10H10 has yielded two interconvertible isomers Os3(CO)9(μ3‐4,5,9‐C2B10H8)(μ‐H)2 (1 a) and Os3(CO)9(μ3‐3,4,8‐C2B10H8)(μ‐H)2 (1 b) formed by the loss of the two NCMe ligands and one CO ligand from the Os3 cluster. Two BH bonds of the o‐C2B10H10 were activated in its addition to the osmium cluster. A second triosmium cluster was added to the 1 a/1 b mixture...
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