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Singly linked and vinyl‐linked dimers of dithienothiophenes exhibit different electronic behaviors. Single crystals of the singly linked dimer show a high conductivity of 0.265 S cm−1, five orders of magnitude higher than that of the vinyl‐linked dimer. The huge increase in the hole density of singly linked dimers results from the formation of radicals, which can be reversibly tuned by facile thermal...
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