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The crystal structures of 4 ligand‐rotational isomers of Au25(PET)18 are presented. Two new ligand‐rotational isomers are revealed, and two higher‐quality structures (allowing complete solution of the ligand shell) of previously solved Au25(PET)18 clusters are also presented. One of the structures lacks an inversion center, making it the first chiral Au25(SR)18 structure solved. These structures combined...
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