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Exfoliation of layered structures such as MoS2 (exemplified here by layered structure of Antelope Canyon, USA) strongly depends on the intercalator used. As found by M. Pumera and co‐workers on page 605, n‐Bu‐Li and t‐Bu‐Li produce a more efficient exfoliation of MoS2 than Me‐Li. Exfoliation with n‐Bu‐Li and t‐Bu‐Li gives rise to MoS2 sheets more catalytic for the hydrogen evolution reaction than...
MoS2 and other transition metal dichalcogenides (TMDs) have recently gained a renewed interest due to the interesting electronic, catalytic, and mechanical properties which they possess when down‐sized to single or few layer sheets. Exfoliation of the bulk multilayer structure can be achieved by a preliminary chemical Li intercalation followed by the exfoliation due to the reaction of Li with water...
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