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The ABX3‐type organic‐inorganic hybrid compound CH3NH3ZnI3 is grown by a liquid diffusion method in methylbenzene solution for the first time. The as prepared samples are characterized by single crystal diffraction, XRD, Infrared (IR) and Raman spectra, TG, UV‐Vis and PL respectively. The results indicate that CH3NH3ZnI3 crystal is demonstrated a monoclinic system with the space group P21/n at room...
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