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The preparation of Li 11 BD 4 from Al 11 B 2 , LiD and D 2 and several subsequent hydrogen sorption cycles according to 2LiD+AlB2+3D2↔2LiBD4+Al starting from the desorbed state are investigated by in situ neutron diffraction. Absorption is carried out at T=450° C and at p=50bar D 2 , while desorption is performed at T=450° C using a back-pressure of...
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