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The structures and reactions of different rhodium oxides and dioxygen complexes with RhO4 stoichiometry were investigated by matrix isolation infrared spectroscopy and quantum chemical calculations. The inserted RhO2 molecule reacted with dioxygen upon sample annealing to form the [(η1-O2)RhO2] complex, which can further isomerize to the known [(η2-O2)RhO2] complex via infrared irradiation. Both experimental...
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