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The electrochemical behavior of thin Pd films supported on a Pt(111) electrode is investigated by cyclic voltammetry and in situ Fourier transform infrared (FTIR) spectroscopy. It is demonstrated that in perchloric acid solution underpotential deposition of hydrogen (H upd ) and hydroxyl adsorption (OH ad ) is in strong competition with the adsorption of Cl - ...
The electrochemistry of CO on a bare Pt(111) electrode as well as a Pt(111) electrode modified with pseudomorphic thin palladium films has been studied in alkaline solution by means of Fourier transform infrared (FTIR) spectroscopy. First Pd films were prepared and well characterized in ultra high vacuum and subsequently transferred into the electrochemical cell for the registration of the voltammetric...
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