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Glasses prepared following a sol-gel route must be thermally treated to evacuate solvent and organic radicals. They often undergo phase transitions in the same temperature range where the weight losses occur. When applied to these systems, conventional differential scanning calorimetry (DSC) may lead to deceiving interpretations. In this paper the transformations of a sol-gel lithium triborate glass,...
This paper investigates the potential of the Modulated Differential Scanning Calorimetry (MDSC TM ) technique in the thermal characterisation of various amorphous materials. Inorganic glasses, composites and glass-polymer mixed materials have been investigated in order to separate the glass transition from irreversible phenomena, such as cold crystallisation or residual cure. This new technique...
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