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Effect of crystalline structure, anatase and rutile, on the production of OH and O 2− by TiO 2 photocatalytic reaction was investigated. The OH radical free from the TiO 2 surface was monitored by the fluorescence intensity of 2-hydroxyl terephthalic acid produced by the reaction with terephthalic acid. Superoxide radical was detected by the chemiluminescence probe method...
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