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A convergent synthesis of the entire carbon framework of phoslactomycin B is disclosed. An initial route aimed to create the C‐8 tetrasubstituted stereocentre through regioselective intermolecular coupling between an internal alkyne and an allyl silyl ether, adopting Trost's protocol, followed by [2,3] sigmatropic rearrangement. But this was not successful. In a second approach, a propargylic sulfide...
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