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An antioxidant multilayer structure based on thermoplastic corn starch (TPCS) was developed by means of the electrohydrodynamic process of electrospinning. Firstly, the effect of adding electrospun outer layers made of polycaprolactone (PCL) on the microstructure and barrier properties of a thermoplastic corn starch (TPCS) film was evaluated. Secondly, β‐carotene was encapsulated into PCL matrices...
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