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Synchrotron X-ray diffraction study for single crystals of Eu 3 S 4 has revealed that a Th 3 P 4 -type I43d structure transforms to a charge-ordered I42d one at T c =188.5K. The crystal structures of Eu 3 S 4 at T=300, 180 and 160K were determined in the least-squares refinements with the Mo Kα intensity data. The valence-difference contrast...
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