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The electronically unsaturated dirhenium complex [Re2(CO)8(μ‐H)(μ‐Ph)] (1) has been found to exhibit aromatic C−H activation upon reaction with N,N‐diethylaniline, naphthalene, and even [D6]benzene to yield the compounds [Re2(CO)8(μ‐H)(μ‐η1‐NEt2C6H4)] (2), [Re2(CO)8(μ‐H)(μ‐η2‐1,2‐C10H7)] (3), and [D6]‐1, respectively, in good yields. The mechanism has been elucidated by using DFT computational analyses,...
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