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The decakis(trifluoromethyl)fullerene C1‐C70(CF3)10, in which the CF3 groups are arranged on a para7‐meta‐para ribbon of C6(CF3)2 edge‐sharing hexagons, and which has now been prepared in quantities of hundreds of milligrams, was reacted under standard Bingel–Hirsch conditions with a bis‐π‐extended tetrathiafulvalene (exTTF) malonate derivative to afford a single exTTF2–C70(CF3)10 regioisomer in 80...
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