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A novel twist: The UIII complex [((AdArO)3N)U] reacts with CS2 by reductive coupling to form the tetrathiooxalate complex [{((AdArO)3N)U}2(μ‐κ2:κ2‐C2S4)] with a newly formed CC bond (see scheme). The UIV/UIV tetrathiooxalate complex features a nonplanar C2S42− unit in an unprecedented μ‐κ2:κ2 binding mode. Further reduction gives the ethylenetetrathiolate complex [Na(dme)3]2[{((AdArO)3N)U}2(μ‐C2S...
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