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Hydrothermal LiFePO4 has been successfully synthesized using iron powder as an iron source and as an in situ reducing agent. The 100% atom economy delivered by iron metal (Fe0) makes this process green and inexpensive. A plausible mechanism for the formation of hydrothermal LiFePO4 powder is also proposed. The structure of the LiFePO4 powder is well characterized by X-ray diffraction, scanning electron...
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