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Fifteen neutral long‐chain‐substituted discotic nickel bis(1,2‐diphenyl‐1,2‐ethenedithiolene) complexes [Ni(dpedt)2], including thirteen new compounds, have been synthesized by new short and efficient synthetic pathways. Physical investigations show that these complexes are thermally stable, possess good electron‐accepting properties, and absorb light strongly in the near‐infrared spectral region...
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