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Single crystals of the FeII metal‐organic framework (MOF) with 1,3,5‐benzenetricarboxylate (BTC) as a linker were solvothermally obtained under air‐free conditions. X‐ray diffraction analysis of the crystals demonstrated a structure for FeII‐MOF analogous to that of [Cu3(BTC)2] (HKUST‐1). Unlike HKUST‐1, however, the FeII‐MOF did not retain permanent porosity after exchange of guest molecules. The...
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