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An efficient protocol for the bromolactonization of alkenoic acids is presented that obviates the use of molecular bromine or exogenous bromenium sources. Vanadium (V) oxide catalyzes the in situ oxidation of bromide salts to bromenium (Br + ) in a process mediated by urea–hydrogen peroxide complex. Initial mechanistic investigations indicate that the presence of urea does not accelerate the...
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