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We investigated the self‐assembly process of a Pd4L8 double‐walled square (DWS) from [PdPy*4]2+ (Py*: 3‐chloropyridine used as the leaving ligand on the PdII center) and an organic ditopic ligand by QASAP (quantitative analysis of self‐assembly process). DWS is assembled mainly through three pathways. Within 5 minutes of the self‐assembly, all of the substrates, the metal source and the organic ditopic...
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