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Interaction of ATP with cisplatin in the pH range 1.9-9.5 was studied by NMR. A new complex with the composition Pt(NH 3 ) 2 (ATP) 2 , which formed very slowly after cisplatin was added to ATP solution, was identified by DOSY and long range 1 H 15 N HMQC experiments. In the complex, ATP bound Pt at N7, and the N7 Pt bond showed the nature of kinetically...
NOESY experiments have been performed on adenosine-5'-triphosphate (ATP) in the presence of 1:1 Mg 2+ (MgCl 2 ) at different pH. The results show that H8 H1' and H8 H2' interproton NOE intensities change with pH, with nearly equal intensity at low pH (pH 1.9) and with H8 H2' signal stronger than the H8 H1' signal at higher pH (between 3.7 and 8.5). The H8 H1' and H8 H2'...
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