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The interplay of mechanical grinding and aniline vapor fuming on the fluorescence of the pentiptycene‐anthracene‐pentiptycene π‐conjugated molecules PAP‐Cn, where n is 4, 8, 12, or 16 and refers to the number of carbon atom in the terminal alkyl chains, in solid films are reported. The differences and similarities among the four homologs have led to a conclusion of the formation of an emissive triplex...
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