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In this account, we show that intermolecular hypervalent I(III)⋯O interactions play an essential role in the complexation of organo-λ 3 -iodanes with crown ethers. In addition to the well-known driving force for the complexation of crown ethers, ion–dipole interaction, and hydrogen bonding interaction, our result provides a new class of interaction in supramolecular chemistry of crown ethers...
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