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We describe a novel Binol‐containing macrocycle that behaves as a chiroptical probe for the detection of biologically relevant ions (Cu2+, Zn2+) under physiological conditions. The macrocycle synthesis is carried out with Binol‐based synthons suitably derivatized in the 2,2′‐ and 3,3′‐positions, by means of a room temperature esterification reaction as the cyclization procedure, followed by late‐stage...
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