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Tuning the nanoclusters’ compositions and structures is critical for the performance improvement of nanoclusters. Herein, a well‐known Au25(SCH2CH2Ph)18 (Au25 for short) nanocluster has been transformed to a rare cadmium doped gold nanocluster [Au13Cd2(PPh3)6(SC2H4Ph)6(NO3)2]2Cd(NO3)4 (Au26Cd5 for short) by peeling and doping. Although Au25 exhibits no catalytic activity toward A3‐coupling reaction...
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