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p-Methoxybenzylidene-assisted intramolecular aglycon delivery was developed in this laboratory and has been demonstrated to be highly efficient and versatile particularly for the synthesis of complex glycoprotein-related glycans. It was revealed that the reaction course of IAD can be clearly monitored by performing the reaction in an NMR tube. Our results suggest that the nonhydrolytic pathway that...
Synthesis of a core heptasaccharide asparagine N 4 -{α-d-mannopyranosyl-(1→6)-[(α-d-mannopyranosyl)-(1→3)]-[(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(1→2)]-(β-d-mannopyranosyl)-(1→4)-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(1→4)-[(α-l-fucopyranosyl)-(1→6)]-2-acetamido-2-deoxy-β-d-glucopyranosyl}-l-asparagine (1a) found from CHO glycosylation mutant cell LEC 14 is described. The structure...
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