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Oxidation of Co 2 (DPhF) 3 or hydrolysis of Co 2 (DPhF) 4 (DPhF = N,N -diphenylformamidinate) gives Co 4 O(DPhF) 6 (I). This tetranuclear compound consists of an oxygen atom centered in a tetrahedron of four-coordinate Co atoms with a DPhF bridge along each edge of the tetrahedron. An idealized T d symmetry is also found for zinc, II, and...
The syntheses, crystal and molecular structures of eight transition metal compounds possessing ligands of the type [(p-tol)-NC(H)N(p-tol)] - (DTolF), [(phenyl)NC(H)N(phenyl)] - (DPhF), and the corresponding triazenato ligands [(phenyl)NNN(phenyl)] - (DPhTA) are presented. Common to all of the compounds is a homoleptic tris-chelated structure with virtual D 3 symmetry...
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