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The six‐vertex closo‐1‐SeB5Cl5 (1) and the 12‐vertex closo‐1‐SeB11Cl11 (2) selenaboranes were prepared in low yields from the co‐pyrolysis reaction of B2Cl4 with Se2Cl2 at 330 °C. Both compounds are sublimable, colorless solids and were tentatively characterized by 11B NMR and high‐resolution mass spectroscopy. DFT/GIAO/NMR calculations support octahedral and icosahedral arrangements for 1 and 2,...
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