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Caging cages: Crystals of a metal‐organic framework, MOF‐123 [Zn7O2(NBD)5(DMF)2] have a three‐dimensional porous structure in which DMF ligands (see picture, pink) protrude into small channels. Removal of these ligands triggers the transformation of this MOF to the doubly interpenetrating form, MOF‐246 [Zn7O2(NBD)5]. Moreover, addition of DMF into MOF‐246 triggers reverse transformation to give MOF‐123...
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