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The β-diketimine (Ph2-nacnac)H [(Ph2-nacnac)=HC{C(Me)NPh}2] reacts with one equivalent of MH3·NMe2Et to produce the corresponding metal dihydride compound (Ph2-nacnac)MH2 [M=Al(1), Ga(2)] by release of hydrogen. Compounds 1 and 2 do not react with a second equivalent of (Ph2-nacnac)H even at elevated temperature. However, a single step 1:2 reaction of AlH3·NMe2Et and (Ph2-nacnac)H affords a complex...
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