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The 1,4,7,10‐tetrazacyclodecane‐1,4,7,10‐tetraacetic acid (DOTA) aqueous complex of UIV with H2O, OH−, and F− as axial ligands was studied by using UV/Vis spectrophotometry, ESI‐MS, NMR spectroscopy, X‐ray crystallography, and electrochemistry. The UIV–DOTA complex with either water or fluoride as axial ligands was found to be inert to oxidation by molecular oxygen, whereas the complex with hydroxide...
The complex [BuMeIm] 2 [UCl 6 ] was characterized in the solid state and in a solution of [BuMeIm][Tf 2 N] room temperature ionic liquid using single-crystal XRD, EXAFS, visible absorption spectroscopy and NMR techniques.The structure of solid [BuMeIm] 2 [UCl 6 ] contains two crystallographically independent formula units (U(1) and U(2)).The U–Cl distances in...
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