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The synthesis, characterization, and stability study of the first uranium complex bearing 2,6-diacetylpyridine dioxime (dapdoH2) is reported. The dimeric complex [UO2(dapdoH)Cl]2 is stable in solution as shown by ESI-MS and NMR spectrometry, and its solid-state structure was further analyzed by X-ray crystallography, IR, Raman and luminescence studies.
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