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In recent years, X‐ray emission spectroscopy (XES) in the Kβ (3p‐1s) and valence‐to‐core (valence‐1s) regions has been increasingly used to study metal active sites in (bio)inorganic chemistry and catalysis, providing information about the metal spin state, oxidation state and the identity of coordinated ligands. However, to date this technique has been limited almost exclusively to first‐row transition...
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