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Support framework: Post‐synthesis modification of an interpenetrating Zn‐based chiral metal–organic framework with Ti(OiPr)4 results in a Lewis acidic catalyst (see picture; gray C, white H, red O, green Ti) with modest enantioselectivity in the asymmetric addition of diethylzinc to aldehydes. The Ti(OiPr)4‐treated framework contains single‐crystal to single‐crystal cross‐linking of the two interpenetrating...
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