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New reduction method for preparation of coordination fullerene complexes is developed. NiII(Me3P)2Cl2 reduction with sodium amalgam in N,N′-dimethylformamide produces reduction products whose interaction with fullerenes C60 and C70 produces coordination complexes which have been crystallized as Ni(Me3P)3(η2-C60) (1) and Ni(Me3P)3(η2-C70) (2) by slow mixing with n-hexane. Due to small size of the Me...
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