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Two ways to relax: A defect‐dicubane Co2Dy2 single‐molecule magnet (SMM) displays slow relaxation of magnetization with a blocking temperature of 22 K (at 1500 Hz), the highest reported for a 3d–4f‐based SMM. Analysis of the relaxation reveals two distinct blocking regimes, one of which is intraionic, localized on the DyIII ions, while the other is exchange‐based.
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