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Fool-proof syntheses of two highly soluble tetraalkylated bicyclic guanidinates which are characterized by the NC(N)N core are reported along with the structures of the corresponding hydrochlorides. The compound with alkyl=methyl was used to prepare a paddlewheel species with a Pd 24+ core devoid of a strong metal–metal bond but potentially useful as precursor to a rare single bonded...
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